XRD Application Systems

In-Situ Flow Electrochemical Cell (ISFEC)

A flow-type electrochemical cell for in-situ and in-operando electrochemical reaction measurements in XRD and accelerator-based analysis environments.

ISFEC is configured to flow a liquid electrolyte or reaction solution through the cell so researchers can observe precursor changes, reaction intermediate formation, and final material generation in real time. It can also be used without fluid flow as a cell for aqueous batteries, electrode reactions, and electrochemical property analysis.

ISFEC physical system with the measurement window and fluid lines connected

Highlights

ISFEC is configured to flow a liquid electrolyte or reaction solution through the cell so researchers can observe precursor changes, reaction intermediate formation, and final material generation in real time. It can also be used without fluid flow as a cell for aqueous batteries, electrode reactions, and electrochemical property analysis.

01

Cell structure for XRD and accelerator-based analysis

02

Supports both Flow and Static measurement modes

03

Three-electrode electrochemical measurement configuration

04

Chemical-resistant materials with Viton O-ring sealing

05

Compact structure integrated with a small stage

Application / Use Case

In-situ / in-operando electrochemical reaction analysis

01

In-situ / in-operando XRD electrochemical analysis

02

Accelerator-based electrochemical reaction analysis

03

Real-time observation of precursor reactions and material formation

04

Aqueous battery and electrode reaction analysis

05

Electrochemical reaction studies under electrolyte flow conditions

06

Reaction mechanism analysis for catalysts, electrode materials, and energy materials

07

Liquid-phase reaction analysis using a flow-cell configuration

ISFEC physical system with the measurement window and fluid lines connected

Technical Highlights

ISFEC is configured to flow a liquid electrolyte or reaction solution through the cell so researchers can observe precursor changes, reaction intermediate formation, and final material generation in real time. It can also be used without fluid flow as a cell for aqueous batteries, electrode reactions, and electrochemical property analysis.

Measurement Concept

Measurement Concept

Designed to perform electrochemical reactions and X-ray analysis at the same time, enabling linked analysis of structural changes and electrochemical signals during reaction.

Operating Modes

Operating Modes

Flow mode supports observation of precursor, reaction intermediate, and product changes under liquid-flow conditions. Static mode supports use as an aqueous battery or general electrochemical cell without fluid flow.

Electrode Configuration

Electrode Configuration

Based on a three-electrode system with Working Electrode, Counter Electrode, and Reference Electrode. Electrode specifications can be changed by experiment purpose.

Material / Sealing

Material / Sealing

Uses Aluminum, Stainless Steel, PI, PEEK, and Viton O-ring sealing to account for structural rigidity, corrosion resistance, insulation, chemical resistance, and leak prevention.

Optional Specs

A flow-type electrochemical cell for in-situ and in-operando electrochemical reaction measurements in XRD and accelerator-based analysis environments.

Product NameIn-Situ Flow Electrochemical Cell
PurposeIn-situ / in-operando electrochemical measurement for XRD and accelerator applications
Measurement ModesFlow mode / Static mode
Analysis ScopePrecursor reaction observation, material formation observation, aqueous battery property analysis
Electrode ConfigurationThree-electrode system
Working ElectrodeAFE5T050GC, PINE
Counter ElectrodeCE-200, EC-Frontier
Reference ElectrodeMiniHydroflex, Gaskatel
Electrode ChangesAvailable on request
DimensionsW112 x D70 x H99 mm, including stage
Weight600 g or more, including stage
Main MaterialsAluminum, Stainless Steel, PI, PEEK
Sealing MethodO-ring
O-ring MaterialViton
Applicable FluidsLiquid electrolyte / reaction solution
ApplicationsIn-situ XRD, in-operando analysis, electrochemical reaction analysis, aqueous battery analysis

Product Inquiry

Align equipment scope with experiment conditions

Discuss installation constraints, sample formats, and test conditions in the same workflow.